brilliant ideas

Freeze dryer info

When ice sublimates in a vacuum (that’s the process where by ice goes directly to water vapor without first melting), it requires heat (just like when you sweat and the sweat evaporates, the process of evaporation removes heat thereby cooling your body). This causes the ice to get colder and colder until it’s so much colder than the surrounding environment that the radiant heat being transferred to the ice equals the amount of heat being consumed by the sublimation process. I’ve seen this effect cause the ice in the freeze dryer to go from being about -5′C down to about -45′C. If you can add additional heat via the heating coils, then the ice stays warmer and sublimates faster. I was worried because the lowest setting for the heater thermostats on the freeze dryer is 60′F (about 15′C). I was afraid that the thermostats wouldn’t allow me to set the temp any lower, and that a temp this high would actually add so much heat that it would cause the ice to melt before it sublimated and thereby screw up the freeze drying process. As it turns out, even though 60′F is the first mark on the thermostats, if you don’t turn them all the way up to that first mark, they still work and they will allow you to set the temperature lower than that. They actually go all the way down to about 23′F (or -5′C). So, I set the thermostats to about 40-50′F (6-10′C), which is above freezing, but due to the laws of thermodynamics and heat transfer principles, the shelf can be slightly above freezing and still not transfer enough heat to the ice to cause it to melt. By being able to set the heat to this setting and then just leave the heat turned on all the time (versus going out once an hour to turn the heat on for 5 minutes or so just to rewarm the shelves from -25′C up to about 0′C), I should be able to speed the drying process. I’m hoping to get the total drying time down from roughly 48 hours to 24 hours. If I can, then I both half my costs per batch, and double my annual capacity (assuming the machine is kept running 24/7). This is important because I can only get somewhere around 2,000 to 8,000 pills worth of product per batch, and with a dosage of 3 to 4 pills per day per, that’s not a whole lot of production capacity should this business take off. So, the faster I can run stuff through, the longer we can make do with this freeze dryer before I have to build the custom freeze dryer I’ve been designing in my mind. BTW, when I’m done building that custom freeze dryer, I’m going to name the specific method of freeze drying that it uses the “Ledford Method” of freeze drying. I’m such an egomaniac ;-)

Freeze drying

I started another run last night. Only a partial run, 1 tray out of the 4 is all that’s in use (although it was pretty full). I’m controlling the method in which this tray is dried in order to provide a control for some experiments. Although it’s not done yet, I can say with confidence that one of the ideas I had for a freeze dryer is current a definite win and something that will improve the process significantly. If I get to, I’m going to name my method of freeze drying the “Ledford Method” :-D

Been quiet lately

It’s not my fault though, I swear. You see, ryeth normally posts about all the day to day things, so I don’t duplicate what she does. That means I only post about unique goings on around our house (or scientific/social diatribes). But, due to our fucked up patent system in America, if you tell people about what you are working on before you patent it, you loose the right to patent it (tell people in a public sense, you can tell individuals privately, but mass dissemination is out). Well, I’m working on some research in my spare time, and some of it appears to possibly be patentable, so I can’t talk about it. That’s why I’ve been so quite lately. However, I can say that I’m now able to freeze dry small samples of things at my home and I can say that I think I’ve come up with a design for equipment that will simplify the mechanical requirements of freeze drying. I just can’t say *how* my design does so or that would kill the patentable part of it ;-)

Food idea…

So, a little while back, Ryeth posted about interesting foods. This one is *very* simple, but also *very* good ;-)

Toast some bread. Let it sit to cool off. Once it’s cool enough that it *won’t* melt the butter, butter the bread (a good thick coat is better). If the bread’s too hot, the butter melts and the bread gets soggy. That’s bad. Next get out some good jelly (I used Strawberry Preserves tonight) and put that over the butter. Then eat. It’s good ;-)